2,3,5,6-四氟苯硫酚合成路线 (共 10 条)
反应条件
potassium hydrosulphide in N,N-dimethyl-formamide T=45 - 55°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 11 p. 1647 - 1653
反应条件
in pyridine; ethylene glycol
参考文献
Journal of the Chemical Society, , p. 4754 - 4760
NL6605036 , ;
C.A., , vol. 66, p. 65492
反应条件
(i) nBuLi, (ii) sulfur; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 865 - 869
参考文献
Butler, Paul F.; Peach, Michael E.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 489 - 496
反应条件
bromine T=500 - 510°C;
参考文献
Platonov; Maksimov; Dvornikova; Nikul'shin
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 11 p. 1647 - 1653
反应条件
bromine T=500 - 510°C;
参考文献
Platonov; Maksimov; Dvornikova; Nikul'shin
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 11 p. 1647 - 1653
反应条件
chlorine T=400°C; 0.305 h;
参考文献
Platonov; Maksimov; Dvornikova; Nikul'shin
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 11 p. 1647 - 1653
反应条件
in diethyl ether; hexane
at -70°C after acidification with 6 N HCl;
参考文献
Tamborski,C.; Soloski,E.J.
Journal of Organic Chemistry, 1966 , vol. 31, p. 746 - 749
反应条件
C4H9Li; CO2
hydrolysis;
参考文献
Brooke,G.M.; Quasem,M.A.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 865 - 869
反应条件
(i) nBuLi, (ii) /BRN= 1900390/; Multistep reaction;
参考文献
Brooke,G.M.; Quasem,M.A.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 865 - 869