2,3,5,6-四氟苯酚合成路线 （共 20 条）
反应条件
(i) (CF3SO3)3Tl, (ii) aq. NaI; Multistep reaction;
参考文献
Australian Journal of Chemistry, , vol. 32, p. 737 - 753
反应条件
(i) (heating), KOH, (ii) (decarboxylation); Multistep reaction;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 10, # 2 p. 344 - 350,343 - 348
反应条件
1: (thermolysis) 2: (i) (heating), KOH, (ii) (decarboxylation) View Scheme
参考文献
Zhurnal Organicheskoi Khimii, , vol. 10, # 2 p. 344 - 350,343 - 348
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
反应条件
dicyclohexyl-carbodiimide in tetrahydrofuran T=20°C;
参考文献
Wilson, Hanna
Journal of Labelled Compounds and Radiopharmaceuticals, 2003 , vol. 46, # 6 p. 511 - 513
反应条件
1: boron trifluoride etherate / 48 h / Heating 2: 70 percent / Et3N / acetonitrile / 20 °C View Scheme
参考文献
Josse, Olivier; Labar, Daniel; Georges, Benoit; Gregoire, Vincent; Marchand-Brynaert, Jacqueline
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 3 p. 665 - 675
反应条件
1: TFP-OH With n-butyllithium in tetrahydrofuran; hexane T=-65°C; 1 h; 2: carbon dioxide in tetrahydrofuran; hexane T=-65 - 20°C; 3 h;
参考文献
Kang, Seok Ho; Luo, Jingdong; Ma, Hong; Barto, Richard R.; Frank, Curtis W.; Dalton, Larry R.; Jen, Alex K.-Y.
Macromolecules, 2003 , vol. 36, # 12 p. 4355 - 4359
反应条件
2-iodoxybenzoic acid amide resin; tetraethylammonium bromide in dichloromethane T=20°C; 0.5 h;
参考文献
Synlett, , # 2 art. no. U24604ST, p. 279 - 282
参考文献
Budnik,A.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1185 - 1189
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 6 p. 1281 - 1285
反应条件
in further solvent(s)
in SbF5, 70°C, 1 h;
参考文献
Yakobson, G. G.; Furin, G. G.; Terent'eva, T. V.
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, p. 802 - 806
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, p. 799 - 804
