2,3,5,6-四氟苯酚合成路线 （共 20 条）
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in cyclohexane T=50°C;
参考文献
Feldman, David; Segal-Lew, Drorit; Rabinovitz, Mordecai
Journal of Organic Chemistry, 1991 , vol. 56, # 26 p. 7350 - 7354
反应条件
trifluoroacetic acid
参考文献
Journal of Fluorine Chemistry, , vol. 149, p. 82 - 87
反应条件
sodium nitrite in dimethyl sulfoxide T=160 - 170°C; 5 h; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 2.2 p. 317 - 319
Zhurnal Organicheskoi Khimii, , vol. 25, # 2 p. 355 - 357
反应条件
H2SO4, NaNO2, Na2CO3 in sulfuric acid 2 h with NaNO2, added Na2CO3, stirred at 0°C for 2 h, added 70percent H2SO4 and H3PO2, warmed on waterbath for 0.75 h.;
参考文献
Journal of the Chemical Society, , p. 2088 - 2094
反应条件
1: H2O 2: H2SO4, NaNO2, Na2CO3 / sulfuric acid View Scheme
参考文献
F: PerFHalOrg.7, 1, page 1 - 84
反应条件
1: HI 2: H2SO4, NaNO2, Na2CO3 / sulfuric acid View Scheme
参考文献
F: PerFHalOrg.7, 1, page 1 - 84
反应条件
benzophenone; water-d2; sodium 1.) THF, 50 deg C, 2.) aceton-d6; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2856 - 2860
反应条件
hydrogen fluoride 17 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2091 - 2098
反应条件
in water; acetonitrile T=25°C; pH 7.00; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 109, # 21 p. 6362 - 6368
反应条件
sulfuric acid; water 1.) 20 deg C, 2 h; 2.) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 22, p. 345 - 376
