1,3-苯并二氧戊环-4-烷基甲醇合成路线 （共 13 条）
反应条件
sodium dithionite; sodium hydrogencarbonate in 1,4-dioxane; water T=85°C; Reduction; 3 h;
参考文献
Synthetic Communications, , vol. 28, # 12 p. 2253 - 2257
反应条件
1: in tetrahydrofuran T=-10°C; 1 h; 2: With water; ammonium chloride
参考文献
WO2003/72561 A1, ;
Page/Page column 17-18 ;
反应条件
hydrogenchloride in diethyl ether; ethyl acetate
反应条件
aminosulfonic acid; water T=20°C; 0.9 h;
参考文献
Synthetic Communications, , vol. 40, # 10 p. 1500 - 1507
反应条件
sodium tetrahydroborate; potassium carbonate in dichloromethane; water T=0 - 15°C; chemoselective reaction;
参考文献
Synthetic Communications, , vol. 40, # 19 p. 2897 - 2907
反应条件
1: 78 percent / Cs2CO3 / dimethylformamide / 2 h / 110 °C 2: 90 percent / sodium borohydride; aq.NaOH / methanol / 0 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 4 p. 803 - 807
反应条件
baker's yeast on montmorillonite K10; potassium chloride; [14C]-Sucrose T=35°C; Reduction; Bioreduction; 48 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 21 p. 3133 - 3137
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Chemische Berichte, , vol. 91, p. 36,38
反应条件
1: chloroform; sulfuric acid; acetic acid 2: aqueous methanol; sodium-amalgam View Scheme
参考文献
Journal of the Chemical Society, , p. 725
反应条件
1: methanol; diethyl ether 2: lithium alanate; diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 91, p. 36,38
