2,4,6-三甲基苯乙烯合成路线 （共 42 条）
反应条件
biphenyl-2-yl-di-tert-butyl-phosphane; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=40°C; 24 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Journal of the American Chemical Society, 2008 , vol. 130, # 11 p. 3690 - 3704
反应条件
dioxathion; caesium carbonate; palladium dichloride in tetrahydrofuran; water T=85°C; Suzuki-Miyaura reaction; 22 h;
参考文献
Molander, Gary A.; Brown, Adam R.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9681 - 9686
反应条件
cis,cis,cis-tetrakis[(diphenylphosphanyl)methyl]cyclopentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in xylene T=130°C; Suzuki reaction; 20 h;
参考文献
Peyroux, Eugenie; Berthiol, Florian; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2004 , # 5 p. 1075 - 1082
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide; sodium hydroxide in water T=60°C; Hiyama coupling; 8 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Chemical Communications, 2010 , vol. 46, # 47 p. 9046 - 9048
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=1551.49 Torr; 24 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in tetrahydrofuran; water T=150°C; Suzuki-Miyaura coupling; P=7757.43 - 9050.33 Torr; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Brooker, Matthew D.; Cooper Jr., Stefan M.; Hodges, Dena R.; Carter, Rhiannon R.; Wyatt, Justin K.
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6748 - 6752
反应条件
(IMes)CuCl; triphenylphosphine; isopropyl alcohol in 1,4-dioxane; diethyl ether T=60°C; 1 h;
参考文献
Lebel, Helene; Davi, Michael; Diez-Gonzalez, Silvia; Nolan, Steven P.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 144 - 149
反应条件
palladium diacetate; Ipr.HCl; tetrabutyl ammonium fluoride in tetrahydrofuran; 1,4-dioxane T=80°C; 48 h;
参考文献
Grasa, Gabriela A.; Nolan, Steven P.
Organic Letters, 2001 , vol. 3, # 1 p. 119 - 120
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in tetrahydrofuran; water T=85 - 90°C; 168 h;
参考文献
Carter, Rhiannon R.; Wyatt, Justin K.
Tetrahedron Letters, 2006 , vol. 47, # 34 p. 6091 - 6094
反应条件
sulfuric acid Erhitzen unter vermindertem Druck;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 59, p. 629,645
