3,7-二苯基-1,5-二硫杂-2,4,6,8-四氮杂环辛四烯合成路线 (共 10 条)
反应条件
hydrazine; palladium on activated charcoal Ambient temperature;
参考文献
Amin, Mehul; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1989 , # 16 p. 1137 - 1138
反应条件
N,N'-thiobisphthalimide; bis(p-toluenesulfonyl) sulfur diimide in dichloromethane
Ambient temperature;
参考文献
Amin, Mehul; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1989 , # 16 p. 1137 - 1138
反应条件
oxygen in acetonitrile
T=60°C; 3 h;
参考文献
Boere, Rene T.; Moock, Klaus H.; Derrick, Sean; Hoogerdijk, William; Preuss, Kathryn; et al.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 473 - 486
反应条件
SCl2 in toluene
12 h; Ambient temperature;
参考文献
Scholz, Uwe; Roesky, Herbert W.; Schimkowiak, Juergen; Noltemeyer, Mathias
Chemische Berichte, 1989 , vol. 122, p. 1067 - 1070
反应条件
SCl2 in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Scholz, Uwe; Roesky, Herbert W.; Schimkowiak, Juergen; Noltemeyer, Mathias
Chemische Berichte, 1989 , vol. 122, p. 1067 - 1070
反应条件
SCl2; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=0°C;
参考文献
Amin, Mehul; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1989 , # 16 p. 1137 - 1138
反应条件
oxygen; tri-phenyl-antimony in acetonitrile
T=60°C; 1.5 h; other substituted 4-aryl-1,2,3,5-dithiadiazolium salts;
参考文献
Boere, Rene T.; Moock, Klaus H.; Derrick, Sean; Hoogerdijk, William; Preuss, Kathryn; et al.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 473 - 486
参考文献
Amin, Mehul; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1989 , # 16 p. 1137 - 1138
反应条件
in acetonitrile
3 h; Heatingother substituted 4-aryl-1,2,3,5-dithiadiazolium salts;
参考文献
Boere, Rene T.; Moock, Klaus H.; Derrick, Sean; Hoogerdijk, William; Preuss, Kathryn; et al.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 473 - 486
反应条件
1: 75 percent / hydrazine / palladium on charcoal / Ambient temperature
2: 15 percent / sulphur dichloride
View Scheme
参考文献
Amin, Mehul; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1989 , # 16 p. 1137 - 1138