DL-2-氨基丁酸甲酯盐酸盐合成路线 （共 11 条）
反应条件
thionyl chloride T=0 - 20°C;
参考文献
Fuchs, Klaus; Eickmeier, Christian; Heine, Niklas; Peters, Stefan; Dorner-Ciossek, Cornelia; Handschuh, Sandra; Nar, Herbert; Klinder, Klaus
Patent: US2010/144681 A1, 2010 ;
Location in patent: Page/Page column 67 ;
US 20100144681 A1
反应条件
thionyl chloride T=-20 - 20°C;
参考文献
Hildenbrand, Simone; Baqi, Younis; Mueller, Christa E.
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 1 p. 48 - 51
反应条件
hydrogenchloride in methanol; water T=25°C; 24 h;
参考文献
Desrosiers, Jean-Nicolas; Cote, Alexandre; Charette, Andre B.
Tetrahedron, 2005 , vol. 61, # 26 p. 6186 - 6192
反应条件
hydrogen; Pd-BaSO4 in methanol P=2068.6 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4817 - 4820
反应条件
thionyl chloride T=55°C;
参考文献
US2005/182262 A1, ;
Page/Page column 2 ;
反应条件
ammonia in methanol T=100°C; 4 h; Microwave irradiation;
参考文献
Hildenbrand, Simone; Baqi, Younis; Mueller, Christa E.
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 1 p. 48 - 51
反应条件
lithium aluminium tetrahydride
参考文献
Feibush,B. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1979 , p. 1230 - 1236
反应条件
ammonia in methanol T=100°C; 4 h; Microwave irradiation;
参考文献
Hildenbrand, Simone; Baqi, Younis; Mueller, Christa E.
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 1 p. 48 - 51
反应条件
ammonia in methanol T=100°C; 4 h; Microwave irradiation;
参考文献
Hildenbrand, Simone; Baqi, Younis; Mueller, Christa E.
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 1 p. 48 - 51
参考文献
Rosochacka,J.
Roczniki Chemii, 1970 , vol. 44, p. 321 - 327
