反应条件
NaBH4; O2 KI added to Cu-salt with stirring, Ar bubbled for 15 min, NaBH4 added dropwise, stirred for 2.5-3 h, allowed to stand for 6-12 h; decanted, washed with H2O, EtOH, dried in air at 40-60°C;
参考文献
Inorganic Materials, , vol. 48, # 6 p. 630 - 634
