2,2,6,6-四甲基哌啶合成路线 (共 107 条)
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide P=1.5 Torr; 40 h;
参考文献
Wysocka, Waleria
Heterocycles, 1982 , vol. 19, # 1 p. 1 - 5
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl in toluene T=90°C; 3 h;
参考文献
Journal of the American Chemical Society, , vol. 121, # 16 p. 3939 - 3943
反应条件
in sulfuric acid; water
参考文献
Ciba-Geigy Corporation
Patent: US4208525 A1, 1980 ;
反应条件
thiophosgene T=20°C; 24 h;
参考文献
Zakrzewski, Jerzy; Hupko, Jarosllaw; Kryczka, Krzysztof
Monatshefte fur Chemie, 2003 , vol. 134, # 6 p. 843 - 850
反应条件
in toluene T=100°C; 8 h; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic data;
参考文献
Journal of the American Chemical Society, , vol. 121, # 16 p. 3939 - 3943
反应条件
in tert-butyl alcohol T=130°C; 24 h;
参考文献
Canadian Journal of Chemistry, , vol. 81, # 6 p. 697 - 704
反应条件
tert.-butylhydroperoxide; zinc dibromide in pyridine; water T=80°C; 16 h;
参考文献
Wu, Xiao-Feng; Bheeter, Charles Beromeo; Neumann, Helfried; Dixneuf, Pierre H.; Beller, Matthias
Chemical Communications, 2012 , vol. 48, # 100 p. 12237 - 12239
反应条件
sodium periodate; RuO4 in tetrachloromethane; water 5 h;
参考文献
Archiv der Pharmazie, , vol. 317, # 1 p. 21 - 27
反应条件
ethanethiol in benzene Yields of byproduct given;
参考文献
Zakrzewski, Jerzy
Monatshefte fuer Chemie, 1990 , vol. 121, # 10 p. 803 - 808
反应条件
1: [Li(μ-2,2,6,6-tetramethylpiperidide)(μ-bis[2-(N,N-dimethylamino)ethyl]ether)Al(isobutyl)2] With zinc diacetate in tetrahydrofuran Inert atmosphere; 2: para-iodoanisole With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran Inert atmosphere;
参考文献
Campbell, Ross; Crosbie, Elaine; Kennedy, Alan R.; Mulvey, Robert E.; Naismith, Rachael A.; Robertson, Stuart D.
Australian Journal of Chemistry, 2013 , vol. 66, # 10 p. 1189 - 1201