(5-乙基吡啶-2-基)甲醇合成路线 （共 6 条）
反应条件
manganese(IV) oxide in chloroform T=20°C; 18 h;
参考文献
Kureha Corporation
Patent: EP1724263 A1, 2006 ;
Location in patent: Page/Page column 39 ;
参考文献
Carpenter, Donald E.; Imbordino, Rick J.; Maloney, Mark T.; Moeslein, Jeffery A.; Reeder, Michael R.; Scott, Allen
Organic Process Research and Development, 2002 , vol. 6, # 5 p. 721 - 728
反应条件
thionyl chloride in chloroform 2 h; Reflux;
参考文献
Thibon, Aurore; Bartoli, Jean-Franois; Bourcier, Sophie; Banse, Frederic
Dalton Transactions, 2009 , # 43 p. 9587 - 9594
反应条件
1.1: potassium hydroxide 2.1: N-bromosuccinmide; acetic acid / water; tert-butyl alcohol / 1 h / 10 °C / |Inert atmosphere; |Large scale 3.1: sodium hydroxide / toluene; tert-butyl methyl ether / 78 °C / |Inert atmosphere; |Large scale 3.2: 1 h / 38 - 42 °C / |Large scale 4.1: sodium tetrahydroborate; cobalt(II) chloride; dmgH2; sodium hydroxide / water; tetrahydrofuran / 0.5 h / 15 - 20 °C 4.2: 15 - 20 °C / pH Ca. 10 View Scheme
参考文献
Carpenter, Donald E.; Imbordino, Rick J.; Maloney, Mark T.; Moeslein, Jeffery A.; Reeder, Michael R.; Scott, Allen
Organic Process Research and Development, 2002 , vol. 6, # 5 p. 721 - 728
反应条件
water; potassium carbonate in dichloromethane
T=20°C;
参考文献
Thibon, Aurore; Bartoli, Jean-Franois; Bourcier, Sophie; Banse, Frederic
Dalton Transactions, 2009 , # 43 p. 9587 - 9594
参考文献
UNILEVER PLC; UNILEVER N.V.
Patent: EP1001009 A1, 2000 ;
