4-(乙酰氧基)-2-环戊烯-1-酮合成路线 （共 15 条）
反应条件
2: aq. HCl View Scheme
参考文献
Osterthun,V.; Winterfeldt,E.
Chemische Berichte, 1977 , vol. 110, p. 146 - 153
反应条件
chlorine; triethylamine in diethyl ether T=26 - 29°C; 1.5 h; Yield given;
参考文献
Mori, Kenji; Takeuchi, Tadashi
Tetrahedron, 1988 , vol. 44, # 2 p. 333 - 342
反应条件
sulfuric acid in water T=55°C; 12 h;
参考文献
Gerdil, Raymond; Liu, Huiyou; Bernardinelli, Gerald
Helvetica Chimica Acta, 1999 , vol. 82, # 3 p. 418 - 434
反应条件
titanium tetrachloride in dichloromethane 1.) -78 deg C, 20 min, 2.) -25 deg C, 20 h;
参考文献
Synlett, , # SPEC. ISS. p. 881 - 884
参考文献
Ghorpade, Sandeep R.; Bastawade, Kulbhushan B.; Gokhale, Digambar V.; Shinde, Popat D.; Mahajan, Vishal A.; Kalkote, Uttam R.; Ravindranathan
Tetrahedron Asymmetry, 1999 , vol. 10, # 21 p. 4115 - 4122
反应条件
in di-isopropyl ether
T=20°C;
参考文献
O'Byrne, Aisling; Murray, Cian; Keegan, Dearbhla; Palacio, Carole; Evans, Paul; Morgan, Ben S.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 3 p. 539 - 545
参考文献
Teijin Limited
Patent: US4132726 A1, 1979 ;
反应条件
iron(III) chloride
a.) 0 deg C to r.t., 20min, b.) 40 deg C, 30min;
参考文献
Eschler, Bart M.; Haynes, Richard K.; Ironside, Michael D.; Kremmydas, Steve; Ridley, Damon D.; Hambley, Trevor W.
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4760 - 4766
反应条件
silver(I) acetate
5 h; Heating;
参考文献
Gerdil, Raymond; Liu, Huiyou; Bernardinelli, Gerald
Helvetica Chimica Acta, 1999 , vol. 82, # 3 p. 418 - 434
反应条件
1: m-chloroperbenzoic acid (m-CPBA) / CH2Cl2 / 0.5 h / -70 °C
2: 73 percent / FeCl3 / a.) 0 deg C to r.t., 20min, b.) 40 deg C, 30min
View Scheme
参考文献
Eschler, Bart M.; Haynes, Richard K.; Ironside, Michael D.; Kremmydas, Steve; Ridley, Damon D.; Hambley, Trevor W.
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4760 - 4766
