3-吡嗪羧酰胺 1-氧化物合成路线 (共 16 条)
反应条件
1: phosphorus oxychloride 2: 30percent aq.hydrogen peroxide, 2 M aq. NaOH / pH 9 View Scheme
参考文献
Dlabal, Karel; Palat, Karel; Lycka, Antonin; Odlerova, Zelmira
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 10 p. 2493 - 2501
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
trichlorophosphate 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
1: 70 percent / P4O10 / various solvent(s) / 0.75 h / Heating 2: POCl3 / 0.17 h View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2860 - 2875
反应条件
trichlorophosphate 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2860 - 2875
反应条件
1: 70 percent / P4O10 / various solvent(s) / 0.75 h / Heating 2: POCl3 / 0.17 h View Scheme
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
trichlorophosphate 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
参考文献
BASF SE
Patent: WO2009/112523 A1, 2009 ;
Location in patent: Page/Page column 55 ;
反应条件
trichlorophosphate 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
1: POCl3 2: HCl View Scheme
参考文献
Fujii; Takagi; Seki
Agricultural and Biological Chemistry, 1982 , vol. 46, # 8 p. 2169 - 2172