N-叔丁氧羰基-O-乙基-D-酪氨酸合成路线 （共 7 条）
反应条件
crown ether in benzene 1.5 h;
参考文献
Manning; Olma; Klis; Kolodziejczyk; Seto; Sawyer
Journal of Medicinal Chemistry, 1982 , vol. 25, # 1 p. 45 - 50
反应条件
sodium hydroxide in methanol; water 0.5 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: 1.) K2CO3 / 1.) H2O, 10 min, 2.) t-BuOH, ether, 25 min 2: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 3: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: 88 percent / thionyl chloride / 48 h / Ambient temperature 2: 1.) K2CO3 / 1.) H2O, 10 min, 2.) t-BuOH, ether, 25 min 3: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 4: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 2: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
1: 1.) K2CO3 / 1.) H2O, 10 min, 2.) t-BuOH, ether, 25 min 2: K2CO3, 18-crown-6 / benzene / 1.5 h / Heating 3: NaOH / methanol; H2O / 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 9 p. 1944 - 1946
反应条件
sodium hydride 1.) DMF, 1 h, 10 deg C, 2.) 4.5 h, 10 deg C; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 48, # 22 p. 4127 - 4129
