甲基反式-3-氨基环丁烷羧酸酯合成路线 （共 13 条）
反应条件
hydrogenchloride; palladium 10 on activated carbon; hydrogen in methanol; water P=750.075 Torr; 3 h;
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
1: thionyl chloride / dichloromethane / 1 h / Reflux 2: 1 h / Reflux 3: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C 4: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
1: sulfuryl dichloride 2: pyridine / 18 h / Reflux 3: thionyl chloride / dichloromethane / 1 h / Reflux 4: 1 h / Reflux 5: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C 6: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
1: 1 h / Reflux 2: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C 3: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
1: pyridine / 18 h / Reflux 2: thionyl chloride / dichloromethane / 1 h / Reflux 3: 1 h / Reflux 4: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C 5: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
1: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C 2: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1644 - 1649
反应条件
hydrogenchloride; water 1 h; Reflux;
参考文献
Radchenko, Dmytro S.; Tkachenko, Anton; Grygorenko, Oleksandr O.; Komarov, Igor V.
Synthetic Communications, 2011 , vol. 41, # 11 p. 1644 - 1649
反应条件
hydrogenchloride; palladium 10 on activated carbon; hydrogen in methanol; water
P=750.075 Torr; 3 h;
参考文献
Radchenko, Dmytro S.; Tkachenko, Anton; Grygorenko, Oleksandr O.; Komarov, Igor V.
Synthetic Communications, 2011 , vol. 41, # 11 p. 1644 - 1649
反应条件
1: thionyl chloride / dichloromethane / 1 h / Reflux
2: 1 h / Reflux
3: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C
4: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr
View Scheme
参考文献
Radchenko, Dmytro S.; Tkachenko, Anton; Grygorenko, Oleksandr O.; Komarov, Igor V.
Synthetic Communications, 2011 , vol. 41, # 11 p. 1644 - 1649
反应条件
1: sulfuryl dichloride
2: pyridine / 18 h / Reflux
3: thionyl chloride / dichloromethane / 1 h / Reflux
4: 1 h / Reflux
5: sodium azide / N,N-dimethyl-formamide / 75 h / 100 °C
6: hydrogenchloride; palladium 10 on activated carbon; hydrogen / methanol; water / 3 h / 750.08 Torr
View Scheme
参考文献
Radchenko, Dmytro S.; Tkachenko, Anton; Grygorenko, Oleksandr O.; Komarov, Igor V.
Synthetic Communications, 2011 , vol. 41, # 11 p. 1644 - 1649
