in hydrogen fluoride HF (liquid); under dry Ar in dry box; LiF (0.92 mmol) loaded into FEP react. vessel; SbF5 (8.15 mmol) and anhyd. HF condenced (77 K); stirred (11 d, room temp.); volatiles pumped off (room temp., few h);
参考文献
Benkic, Primoz; Jenkins, H. Donald Brooke; Ponikvar, Maja; Mazej, Zoran
European Journal of Inorganic Chemistry, 2006 , # 5 p. 1084 - 1092