反应条件
in hydrogen fluoride byproducts: NaHF2; HF (liquid); anhyd. HF added to B compd. at -196°C, warmed to room temp., stirred for 1 h, poured at room temp. into NaF, stirred for 10 min; evapd. (vac.), suspended in MeCN, filtered, evapd.; obtained as a mixt.;
参考文献
Inorganic Chemistry, , vol. 43, # 2 p. 490 - 505
