1-(4-溴苯基)吡啶-2-酮合成路线 (共 5 条)
反应条件
copper diacetate; copper(ll) bromide T=120°C; 1 h; Neat (no solvent);
参考文献
Bedford, Robin B.; Engelhart, Jens U.; Haddow, Mairi F.; Mitchell, Charlotte J.; Webster, Ruth L.
Dalton Transactions, 2010 , vol. 39, # 43 p. 10464 - 10472
反应条件
potassium phosphate; (tris(3,5-dimethylpyrazolyl)methane)CuI in 1,4-dioxane T=110°C; Goldberg reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Haldon, Estela; Alvarez, Eleuterio; Nicasio, M. Carmen; Perez, Pedro J.
Inorganic Chemistry, 2012 , vol. 51, # 15 p. 8298 - 8306
反应条件
copper(l) iodide; cesium fluoride; N-methyl-2-(methylamino)ethylamine in tetrahydrofuran T=25°C; 18 - 24 h; Inert atmosphere;
参考文献
Phillips, Dean P.; Zhu, Xue-Feng; Lau, Thomas L.; He, Xiaohui; Yang, Kunyong; Liu, Hong
Tetrahedron Letters, 2009 , vol. 50, # 52 p. 7293 - 7296
反应条件
N-bromosuccinmide; acetic acid; palladium diacetate T=100°C; 12 h;
参考文献
Tetrahedron, , vol. 62, # 49 p. 11483 - 11498
反应条件
Bei der elektrochemischen Reduktion.;
参考文献
Fysiograf.Saellsk.Lund Foerh., , vol. 23, p. 88,90