1.1: 74 percent / KMnO4; Na2CO3 / H2O / 50 h / 50 °C 2.1: 99 percent / NH2OH*HCl / H2O / 0.33 h / 45 °C 3.1: 93 percent / Zn / acetic acid / 0.5 h / 20 - 30 °C 4.1: SOCl2 / methanol / 20 h / 20 °C 5.1: K2CO3; NH2OH*HCl / dioxane; H2O / 12 h / 20 °C 5.2: 18.5 g / 3-dimethylaminopropylamine / dioxane; H2O / 1 h / 20 °C 6.1: 43 percent / McIlvaine's buffer cont. EDTA; thiothreitol / papain (from Carica papaya) / acetonitrile; dimethylformamide / 36 h / 20 °C / pH 6.2 / Enzymatic reaction 7.1: 81 percent / conc. HCl / methanol / 8 h / Heating View Scheme
参考文献
Parker, William L.; Hanson, Ronald L.; Goldberg, Steven L.; Tully, Thomas P.; Goswami, Animesh
Organic Process Research and Development, 2012 , vol. 16, # 3 p. 464 - 469
1.1: 74 percent / KMnO4; Na2CO3 / H2O / 50 h / 50 °C 2.1: 99 percent / NH2OH*HCl / H2O / 0.33 h / 45 °C 3.1: 93 percent / Zn / acetic acid / 0.5 h / 20 - 30 °C 4.1: SOCl2 / methanol / 20 h / 20 °C 5.1: K2CO3; NH2OH*HCl / dioxane; H2O / 12 h / 20 °C 5.2: 18.5 g / 3-dimethylaminopropylamine / dioxane; H2O / 1 h / 20 °C 6.1: 43 percent / McIlvaine's buffer cont. EDTA; thiothreitol / papain (from Carica papaya) / acetonitrile; dimethylformamide / 36 h / 20 °C / pH 6.2 / Enzymatic reaction 7.1: 81 percent / conc. HCl / methanol / 8 h / Heating View Scheme
参考文献
Parker, William L.; Hanson, Ronald L.; Goldberg, Steven L.; Tully, Thomas P.; Goswami, Animesh
Organic Process Research and Development, 2012 , vol. 16, # 3 p. 464 - 469
