反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane Pd(PPh3)4 added to soln. of acetylene and Ph3SnH in CH2Cl2 under Ar, stirred at 25°C for 5 h, poured into water; combined yield 77percent, isomeric ratio 11:82:7; extd. with ethyl acetate, dried (Na2SO4), evapd., preparative TLC on SiO2;
参考文献
Ichinose, Yoshifumi; Oda, Hiroji; Oshima, Koichiro; Utimoto, Kiitiro
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3468 - 3470