3-乙基-2-硫代-4-噻唑烷二酮合成路线 （共 38 条）
反应条件
1: carbon disulfide; ethylamine With sodium hydroxide in water T=100°C; Microwave irradiation; 2: chloroacetic acid in water T=100°C; 0.0833333 h; Microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.5 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 53, # 39 p. 5197 - 5201
反应条件
in methanol; water T=100°C; 4 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 45, # 7 p. 2748 - 2752
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 34, p. 2999 - 3005,3036 - 3041
反应条件
water Ansaeuern des Reaktionsgemisches mit Schwefelsaeure oder Essigsaeure;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 81, p. 456
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>84, p. 665
参考文献
v. Rintelen; Riester
Mitt. Forschungslabor. AGFA, 1955 , vol. 1, p. 65,71, 75
反应条件
triethylamine in pyridine
参考文献
Tolmachev,A.I. et al.
Doklady Chemistry, 1967 , vol. 177, p. 1136 - 1139
Doklady Akademii Nauk SSSR, 1967 , vol. 177, p. 869 - 872
参考文献
Brooker et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5326,5330
反应条件
sodium acetate; acetic anhydride in acetic acid 0.5 h; Heating;
参考文献
Allan,F.J.; Allan,G.G.
Journal of Heterocyclic Chemistry, 1970 , vol. 7, p. 1091 - 1094
反应条件
1: KOAc, Ac2O / acetic acid; heptane / Heating 2: KOAc, Ac2O / acetic acid / 1 h / Heating View Scheme
参考文献
Allan,F.J.; Allan,G.G.
Journal of Heterocyclic Chemistry, 1970 , vol. 7, p. 1091 - 1094
