2,5-二甲基-2,4-己二烯合成路线 （共 127 条）
反应条件
silver perchlorate in benzene T=40.1°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 94, # 22 p. 7780 - 7788
反应条件
biphenyl in acetonitrile T=10°C; 26 h; Irradiation;
参考文献
Canadian Journal of Chemistry, , vol. 72, # 2 p. 415 - 429
反应条件
iron (III) acetylacetonate; Nitrous oxide in tetrahydrofuran T=20°C; 1 h; Schlenk techniqueGlovebox; Reagent/catalyst;
参考文献
Kiefer, Gregor; Jeanbourquin, Loic; Severin, Kay
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6302 - 6305
Angew. Chem., 2013 , vol. 125, # 24 p. 6422 - 6425
反应条件
aluminum oxide; phosphoric acid T=250°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 26, p. 275; engl. Ausg. S. 293
US2715649 , ;
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 1.) 0 deg C, 30 min, 2.) reflux, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 17 p. 4128 - 4131
反应条件
in diethyl ether T=-60°C; Condensation; hydrolysis;
参考文献
Tetrahedron, , vol. 56, # 21 p. 3373 - 3383
反应条件
in pentane Irradiation; Yield given. Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 4556
反应条件
in diethylene glycol dimethyl ether T=160°C; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 23, # 21 p. 2163 - 2166
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 1.) 0 deg C, 30 min, 2.) reflux, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 17 p. 4128 - 4131
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether T=-80°C; Condensation; hydrolysis;
参考文献
Tetrahedron, , vol. 56, # 21 p. 3373 - 3383
