2,5-二甲基-2,4-己二烯合成路线 (共 127 条)
反应条件
anhydrous calcium phosphate T=400°C;
参考文献
Gevo, Inc.
Patent: US2012/271082 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
NiBr2(PPh3)2; triphenylphosphine; zinc in acetonitrile T=20°C; 6 h;
参考文献
Sasaki, Ken; Nakao, Kikuji; Kobayashi, Yoshihiko; Sakai, Mutsuji; Uchino, Norito; et al.
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 8 p. 2446 - 2448
反应条件
1: Me2C=CHMgX With indium(III) chloride in tetrahydrofuran T=20°C; 1 h; 2: 6-acetoxy-1-cyclohexene-1-carbonitrile With triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran
参考文献
Baker, Lucas; Minehan, Thomas
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3957 - 3960
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Walborsky, H. M.; Wuest, H. H.
Journal of the American Chemical Society, 1982 , vol. 104, # 21 p. 5807 - 5808
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Walborsky, H. M.; Wuest, H. H.
Journal of the American Chemical Society, 1982 , vol. 104, # 21 p. 5807 - 5808
反应条件
niobic acid T=220°C; Prins Reaction; P=31029.7 Torr;
参考文献
US2012/271082 A1, ;
Page/Page column 6 ;
反应条件
niobic acid T=225°C; Prins Reaction; P=31029.7 Torr;
参考文献
US2012/271082 A1, ;
Page/Page column 7 ;
反应条件
toluene-4-sulfonic acid
参考文献
Journal of the Science of Food and Agriculture, , vol. 2, p. 94,99
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Walborsky, H. M.; Wuest, H. H.
Journal of the American Chemical Society, 1982 , vol. 104, # 21 p. 5807 - 5808
反应条件
niobic acid on graphite T=215 - 300°C; Prins Reaction; P=3620.13 - 4137.29 Torr;
参考文献
US2012/271082 A1, ;
Page/Page column 6 ;