1: 61.2 g / 35percent hydrogen peroxide/HCOOH / 3 h / 0 °C 2: 57.8 g / 50percent aq. NaOH / methanol / 1.67 h / Heating 3: 61.0 g / phosphorus oxychloride / 6 h / 55 °C View Scheme

1: 57.8 g / 50percent aq. NaOH / methanol / 1.67 h / Heating 2: 61.0 g / phosphorus oxychloride / 6 h / 55 °C View Scheme

trichlorophosphate T=55°C; 6 h;