3-甲基-3-丁烯-1-醇合成路线 （共 220 条）
反应条件
aluminum oxide
T=20°C; 20 h;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
Hg(OTf)2 in nitromethane
T=-20°C; 1 h; Yield givenFurther byproducts given;
参考文献
Nishizawa; Shigaraki; Takao; Imagawa; Sugihara
Tetrahedron Letters, 1999 , vol. 40, # 6 p. 1153 - 1156
反应条件
1: Et3N
2: TMSOTf / CCl4 / 25 °C
View Scheme
参考文献
Mekhalfia; Marko; Adams
Tetrahedron Letters, 1991 , vol. 32, # 36 p. 4783 - 4786
反应条件
aluminum oxide
T=20°C; 20 h;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
toluene-4-sulfonic acid in benzene
T=20 - 25°C; 20 h; Product distributionMechanism;
参考文献
Gevorkyan, A.A.; Arakelyan, A.S.; Kazaryan, P.I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 12 p. 1240 - 1242
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 12 p. 1611 - 1613
反应条件
aluminum oxide
T=20°C; 20 h;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
Hg(OTf)2 in nitromethane
T=-20°C; 1 h; Yield givenFurther byproducts given;
参考文献
Nishizawa; Shigaraki; Takao; Imagawa; Sugihara
Tetrahedron Letters, 1999 , vol. 40, # 6 p. 1153 - 1156
反应条件
Hg(OTf)2 in nitromethane
T=-20°C; 1 h; Further byproducts given;
参考文献
Nishizawa; Shigaraki; Takao; Imagawa; Sugihara
Tetrahedron Letters, 1999 , vol. 40, # 6 p. 1153 - 1156
反应条件
1: Et3N
2: TMSOTf / CCl4 / 25 °C
View Scheme
参考文献
Mekhalfia; Marko; Adams
Tetrahedron Letters, 1991 , vol. 32, # 36 p. 4783 - 4786
反应条件
[Ru(PnOct3)4(H)2]
T=120°C; 20 h; RefluxInert atmosphereSchlenk technique;
参考文献
BASF SE; The designation of the inventor has not yet been filed
Patent: EP2597081 A1, 2013 ;
Location in patent: Paragraph 0124 ;
