顺式-3,3A,4,5-四氢-2-乙酰基-5-((4-甲基苯基)磺酰基)-3-苯基-2H-吡唑并(4,3-c)喹啉合成路线 （共 4 条）
反应条件
1: 97 percent / pyridine / 1) cooling, 15 min, 2) reflux, 30 min
2: 92 percent / 10 percent KOH / methanol; H2O / 4 h / Ambient temperature
3: PCl5
4: 86 percent / AlCl3 / or SnCl4
5: 94 percent / NaOCH3 / methanol / 4 h / Ambient temperature
6: 91 percent / NH2NH2*H2O / acetic acid / 8 h / Heating
View Scheme
参考文献
Kelkar, Prabhakar M.; Sangwan, Naresh K.; Rastogi, Shri Nivas; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 297 - 300
反应条件
1: 94 percent / NaOCH3 / methanol / 4 h / Ambient temperature
2: 91 percent / NH2NH2*H2O / acetic acid / 8 h / Heating
View Scheme
参考文献
Kelkar, Prabhakar M.; Sangwan, Naresh K.; Rastogi, Shri Nivas; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 297 - 300
反应条件
1: PCl5
2: 86 percent / AlCl3 / or SnCl4
3: 94 percent / NaOCH3 / methanol / 4 h / Ambient temperature
4: 91 percent / NH2NH2*H2O / acetic acid / 8 h / Heating
View Scheme
参考文献
Kelkar, Prabhakar M.; Sangwan, Naresh K.; Rastogi, Shri Nivas; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 297 - 300
反应条件
1: 71 percent / acetic acid / 15 h / Heating
2: 97 percent / pyridine / 1) cooling, 15 min, 2) reflux, 30 min
3: 92 percent / 10 percent KOH / methanol; H2O / 4 h / Ambient temperature
4: PCl5
5: 86 percent / AlCl3 / or SnCl4
6: 94 percent / NaOCH3 / methanol / 4 h / Ambient temperature
7: 91 percent / NH2NH2*H2O / acetic acid / 8 h / Heating
View Scheme
参考文献
Kelkar, Prabhakar M.; Sangwan, Naresh K.; Rastogi, Shri Nivas; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 297 - 300
