2,6-二甲基-4-(3-硝基苯基)-吡啶-3,5-二羧酸二甲酯合成路线 (共 9 条)
反应条件
molybdenium(VI) oxotetrachloride in acetonitrile
0.0166667 h; Reflux;
参考文献
Lou, Bin-Hui; Chen, Shu-Bin; Wang, Jian; Chen, Ying; Li, Jing-Hua
Journal of Chemical Research, 2013 , vol. 37, # 7 p. 409 - 412
反应条件
1: aq. NH4OAc / H2O / 0.67 h / Heating
2: KMnO4; aq. AcOH / 4 h / Heating
View Scheme
参考文献
Xia, Jing-Jing; Wang, Guan-Wu
Synthesis, 2005 , # 14 art. no. F02305SS, p. 2379 - 2383
反应条件
1: aq. NH4OAc / H2O / 0.67 h / Heating
2: KMnO4; aq. AcOH / 4 h / Heating
View Scheme
参考文献
Xia, Jing-Jing; Wang, Guan-Wu
Synthesis, 2005 , # 14 art. no. F02305SS, p. 2379 - 2383
反应条件
triethylamine in acetonitrile
Irradiation; Quantum yield;
参考文献
Fasani, Elisa; Fagnoni, Maurizio; Dondi, Daniele; Albini, Angelo
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 2037 - 2045
反应条件
sodium hydroxide in ethanol
2 h; Heating;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 82 percent / NaOH / aq. ethanol / 2 h / Heating
2: 99 percent / 1.5 h / Heating; heating in Dowterm
3: 100 percent / aq. H2O2, 30percent / acetic acid / 3 h / Heating
4: 0.5 h / Heating
5: conc. HCl / 1 h / Heating
6: 76 percent / activated manganese dioxide / CHCl3 / 6 h / Heating
7: 95 percent / palladium on charcoal / various solvent(s) / 1 h / 190 °C / heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: KOH / methanol / 18 h / Heating
2: 40percent peracetic acid / ethanol / 3.5 h / Heating
3: 0.08 h / 140 °C
4: 1) KOH 2) 6N HCl / 1) MeOH, reflux, 5 min, 2) 90-100 deg C, 2 h
View Scheme
参考文献
Shibanuma; Iwanami; Fujimoto; et al.
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 9 p. 2609 - 2613
反应条件
1: 82 percent / NaOH / aq. ethanol / 2 h / Heating
2: 99 percent / 1.5 h / Heating; heating in Dowterm
3: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 82 percent / NaOH / aq. ethanol / 2 h / Heating
2: 99 percent / 1.5 h / Heating; heating in Dowterm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856