苄基(4-甲基苯基)氨基甲酸酯合成路线 （共 10 条）
反应条件
T=130 - 170°C; Rate constant;
参考文献
Mukaiyama; Iwanami
Journal of the American Chemical Society, 1957 , vol. 79, p. 73,75
反应条件
Lanthanum nitrate hexahydrate
T=20°C; 0.0666667 h;
参考文献
Chinni Mahesh; Narasimhulu; Srikanth Reddy; Suryakiran; Venkateswarlu
Tetrahedron Letters, 2007 , vol. 48, # 1 p. 55 - 59
反应条件
1: in tetrahydrofuran
T=55°C; 8 h; Inert atmosphere;
2: With water; ammonium chloride in tetrahydrofuran
Inert atmosphere;
参考文献
Yang, Haoran; Huang, Danfeng; Wang, Ke-Hu; Xu, Changming; Niu, Teng; Hu, Yulai
Tetrahedron, 2013 , vol. 69, # 12 p. 2588 - 2593
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Clayden, Jonathan; Farnaby, William; Grainger, Damian M.; Hennecke, Ulrich; Mancinelli, Michele; Tetlow, Daniel J.; Hillier, Ian H.; Vincent, Mark A.
Journal of the American Chemical Society, 2009 , vol. 131, # 10 p. 3410 - 3411
反应条件
copper diacetate; palladium diacetate; potassium iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=120°C; P=760.051 Torr;
参考文献
Guan, Zheng-Hui; Lei, Hao; Chen, Ming; Ren, Zhi-Hui; Bai, Yinjuan; Wang, Yao-Yu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 489 - 496
反应条件
1: carbon dioxide; p-toluidine With tetra-(n-butyl)ammonium iodide; caesium carbonate in N,N-dimethyl-formamide
T=23°C; 1 h;
2: benzyl chloride in N,N-dimethyl-formamide
T=23°C; 12 h;
参考文献
Salvatore, Ralph N; Chu, Feixia; Nagle, Advait S; Kapxhiu, Elona A; Cross, Richard M; Jung, Kyung Woon
Tetrahedron, 2002 , vol. 58, # 17 p. 3329 - 3347
反应条件
[Pd(CH3CN)4](BF4)2 in acetonitrile
T=20°C; aza-Michael addition; 24 h;
参考文献
Wabnitz, Tobias C.; Yu, Jin-Quan; Spencer, Jonathan B.
Chemistry - A European Journal, 2004 , vol. 10, # 2 p. 484 - 493
反应条件
1.1: ethylene dibromide / tetrahydrofuran / |Inert atmosphere; |Heating
1.2: 0.25 h / 20 °C / |Inert atmosphere
1.3: 20 °C / |Inert atmosphere
2.1: tetrahydrofuran / 8 h / 55 °C / |Inert atmosphere
2.2: |Inert atmosphere
View Scheme
参考文献
Yang, Haoran; Huang, Danfeng; Wang, Ke-Hu; Xu, Changming; Niu, Teng; Hu, Yulai
Tetrahedron, 2013 , vol. 69, # 12 p. 2588 - 2593
反应条件
T=130 - 170°C; Rate constant;
参考文献
Mukaiyama; Iwanami
Journal of the American Chemical Society, 1957 , vol. 79, p. 73,75
