N-(肉桂酰)-4-甲氧基苯胺合成路线 （共 19 条）
反应条件
4-(N,N-dimethlyamino)pyridine; sodium hydrogencarbonate in dichloromethane T=20°C;
参考文献
Zhang, Mao; Lu, Xiang; Zhang, Hong-Jia; Li, Na; Xiao, Yu; Zhu, Hai-Liang; Ye, Yong-Hao
Medicinal Chemistry Research, 2013 , vol. 22, # 2 p. 986 - 994
反应条件
potassium carbonate in acetone T=0°C; 0.5 h;
参考文献
Wang, Tai-Chi; Chen, Yeh-Long; Lee, Kuan-Han; Tzeng, Cherng-Chyi
Synthesis, 1997 , # 1 p. 87 - 90
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in tetrahydrofuran; water T=20°C; Pinnick oxidation; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 50, # 26 p. 3436 - 3438
反应条件
isobutyl chloroformate in chloroform; triethylamine 12 h; Ambient temperature;
参考文献
Lugnier; Bruch; Stoclet; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 2 p. 121 - 125
反应条件
1: SOCl2 2: 69.6 percent / diethyl ether / 0.5 h View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 39, # 10 p. 827 - 834
反应条件
1: 1.) toluene-p-sulphonic acid, 2.) hydrogen, sodium borohydride / 2.) 10percent palladium on charcoal / 1.) benzene, 12 h, reflux 2: 60 percent / ethylmagnesium bromide / tetrahydrofuran / 14 h 3: 8 percent / trifluoroacetic acid / 6 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2105 - 2111
反应条件
1: 1.) toluene-p-sulphonic acid, 2.) hydrogen, sodium borohydride / 2.) 10percent palladium on charcoal / 1.) benzene, 12 h, reflux 2: 60 percent / ethylmagnesium bromide / tetrahydrofuran / 14 h 3: 8 percent / trifluoroacetic acid / 6 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2105 - 2111
反应条件
trimethylsilylazide; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride in acetic acid T=60°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 52 p. 12595 - 12599
反应条件
1: 60 percent / ethylmagnesium bromide / tetrahydrofuran / 14 h 2: 8 percent / trifluoroacetic acid / 6 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2105 - 2111
反应条件
triethylamine in tetrahydrofuran 18 h; Heating;
参考文献
Tetrahedron, , vol. 64, # 27 p. 6510 - 6521
