hydrogenchloride in ethanol; water T=50 - 55°C; 22 h;

1: 85 percent / NaClO4 / N,N-dimethyl-acetamide 2: 70 percent / Amberlite IRA-402 (HCO3-), H2O / 192 h / 3 - 4 °C 3: 69 percent / K2CO3 / dimethylformamide / Ambient temperature 4: 61 percent / 0.1 N aq. HCl / 3.5 h / Ambient temperature 5: HCl / ethanol View Scheme

1: 70 percent / Amberlite IRA-402 (HCO3-), H2O / 192 h / 3 - 4 °C 2: 69 percent / K2CO3 / dimethylformamide / Ambient temperature 3: 61 percent / 0.1 N aq. HCl / 3.5 h / Ambient temperature 4: HCl / ethanol View Scheme

hydrogenchloride in ethanol 72 h; Ambient temperature;

1: 85 percent / AcNMe2 / 4 h / Ambient temperature; 2.) H2O, HClO4 2: 70 percent / Amberlite IRA-402 (HClO3-) / H2O 3: 70 percent / K2CO3 / dimethylformamide / 5 h / Ambient temperature 4: 61 percent / 0.1N HCl / H2O / 3.5 h / Ambient temperature 5: HCl / ethanol / 72 h / Ambient temperature View Scheme

1: 70 percent / K2CO3 / dimethylformamide / 5 h / Ambient temperature 2: 61 percent / 0.1N HCl / H2O / 3.5 h / Ambient temperature 3: HCl / ethanol / 72 h / Ambient temperature View Scheme

1: 61 percent / 0.1N HCl / H2O / 3.5 h / Ambient temperature 2: HCl / ethanol / 72 h / Ambient temperature View Scheme

暂无反应条件数据

in N,N-dimethyl acetamide T=42 - 44°C; 3 h;