4,4-二甲基-1-戊烯合成路线 (共 69 条)
反应条件
in diethyl ether T=22°C; P=2585.7 Torr; 3 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 1440
反应条件
Ta(CHCMe3)2(Me)(PMe3)2 T=25°C; P=1551.4 - 2585.7 Torr; 48 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 5752
反应条件
diethyl ether T=-10 - 5°C;
参考文献
Journal of the American Chemical Society, , vol. 55, p. 4558
US2135064 , ;
反应条件
ethanol; zinc T=120°C; im Rohr;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1438
Journal of the American Chemical Society, , vol. 68, p. 1652,1656
反应条件
triphenylphosphine; copper dichloride in tetrahydrofuran T=60°C;
参考文献
Ibragimov, A. G.; Minsker, D. L.; Saraev, R. A.; Dzhemilev, U. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 10 p. 2104 - 2107
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 10 p. 2333 - 2336
反应条件
zinc(II) chloride in dichloromethane T=0°C; 48 h;
参考文献
Dau-Schmidt, Jan-Peter; Mayr, Herbert
Chemische Berichte, 1994 , vol. 127, # 1 p. 205 - 212
反应条件
T=25°C; P=1551.4 - 2585.7 Torr; 0.5 h; Yield given;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 5752
反应条件
sodium iodide in dimethylsulfoxide-d6 T=35 - 45°C; 3 h; Irradiationalso: without NaI, with other then t-BuHgCl tert-butylating reagents (copper or zinc complexes); reactivities relative to Ph2C=CHI, CH2=C(CH3)CH2I and HCCCH2Cl; MechanismProduct distribution;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Wu, Yuh Wern
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4921 - 4927
反应条件
1: sodium borate; diethyl ether 3: potassium acetate; acetic acid anhydride; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 77, p. 3610,3613
反应条件
WH(η5-C5HMe4)(CO3) in benzene-d6 T=140°C; 48 h;
参考文献
European Journal of Inorganic Chemistry, , # 11 p. 1514 - 1520