2,2-二氟-5,5-二甲基-1,3-环己烷二酮合成路线 (共 4 条)
反应条件
XeF2; polystyrene-4-vinylpyridine*BF3; hydrogen fluoride in dichloromethane
20 h; Ambient temperature;
参考文献
Zajc, Barbara; Zupan, Marko
Journal of the Chemical Society, Chemical Communications, 1980 , # 16 p. 759 - 760
反应条件
fluorine in monofluoro-trichloromethane
参考文献
Patrick, Timothy B.; Scheibel, Jeffrey J.; Cantrell, Gary L.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3917 - 3918
反应条件
fluorine in formic acid
T=10 - 15°C; 2 h;
参考文献
Chambers, Richard D.; Greenhall, Martin P.; Hutchinson, John
Journal of the Chemical Society, Chemical Communications, 1995 , # 1 p. 21 - 22
反应条件
fluorine in formic acid
T=0.6°C; 1 h;
参考文献
Chambers, Richard D.; Hutchinson, John; Batsanov, Andrei S.; Lehmann, Christian W.; Naumov, Dimitrii Y.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2271 - 2275