3-(4-甲氧基苯基)-1-(2,4,6-三羟基苯基)丙-1-酮合成路线 （共 6 条）
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal
T=30°C; P=2280 Torr; 0.5 h;
参考文献
Nakamura, Yoshimasa; Watanabe, Shigeo; Miyake, Nobuyuki; Kohno, Hiroyuki; Osawa, Toshihiko
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 11 p. 3309 - 3312
反应条件
hydrogen; acetic acid; palladium on activated charcoal
T=20°C; 4 h;
参考文献
Alam, Sayed; Islam, Azizul
Pakistan Journal of Scientific and Industrial Research, 2003 , vol. 46, # 1 p. 27 - 30
反应条件
1: 0.8 g
2: 0.4 g / H2 / Pd-C / ethyl acetate / 6 h
View Scheme
参考文献
Mizuno, Mizuo; Kojima, Hiroyuki; Tanaka, Toshijuki; Iinuma, Munekazu; Kimura, Rie; et al.
Phytochemistry (Elsevier), 1987 , vol. 26, # 7 p. 2071 - 2074
反应条件
1: 0.8 g
2: 0.4 g / H2 / Pd-C / ethyl acetate / 6 h
View Scheme
参考文献
Mizuno, Mizuo; Kojima, Hiroyuki; Tanaka, Toshijuki; Iinuma, Munekazu; Kimura, Rie; et al.
Phytochemistry (Elsevier), 1987 , vol. 26, # 7 p. 2071 - 2074
反应条件
1: 44 percent / KOH / ethanol / 75 h / 20 °C
2: 40 percent / 3N aq. HCl / methanol / 0.25 h / Heating
3: 40 percent / H2; AcOH / 5 percent Pd/C / 4 h / 20 °C
View Scheme
参考文献
Alam, Sayed; Islam, Azizul
Pakistan Journal of Scientific and Industrial Research, 2003 , vol. 46, # 1 p. 27 - 30
反应条件
aluminium trichloride; nitrobenzene
参考文献
Shinoda; Sato
Yakugaku Zasshi, 1928 , vol. 48, p. 109
Chem. Zentralbl., 1928 , vol. 99, # II p. 1885
