in ethanol -70 to -60°C, storing (120 h), gradual increase of temperature; IR spectroscopy;
参考文献
Titova, K. V.; Loginova, E. N.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1995 , vol. 40, p. 1714 - 1720
Zhurnal Neorganicheskoi Khimii, 1995 , vol. 40, p. 1781 - 1787
in ethanol hydroxylamine soln. freezing and evac. (vac. apparatus), calculated amount of ClO3F addmitting (condn. in reaction flask), reaction mixt. keeping without or with stirring for definite time at given temp. until complete removal of volatile substances; no isolation of individual substances; chem. anal., IR spectroscopy;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 23, p. 634 - 636
Zhurnal Neorganicheskoi Khimii, , vol. 23, p. 1146 - 1149
in neat (no solvent) detected by mass spectroscopy; not isolated;;
参考文献
Dibeler, V. H.; Reese, R. M.; Mann, D. E.
Journal of Chemical Physics, 1957 , vol. 27, p. 176 - 179
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Gmelin Handbook: Cl: SVol.B2, 6, page 326 - 329
Barth-Wehrenalp, G.
J. inorg. nuclear Chem., 1956 , vol. 2, p. 266 - 266
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Woolf, A. A.
J. inorg. nuclear Chem., 1956 , vol. 3, p. 250 - 250
Rohrback, G. H.; Cady, G. H.
Journal of the American Chemical Society, 1947 , vol. 69, p. 677 - 678
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Gmelin Handbook: Cl: SVol.B2, 66, page 462 - 464
