1,1,2-三氯三氟乙烷（CFC-113）合成路线 （共 198 条）
反应条件
1,1,2,2-tetrachloro-1,2-difluoroethane; antimony(V) pentachloride; fluorine T=32°C; unter vermindertem Druck;
反应条件
hydrogen fluoride; cobalt-substituted chromium oxide (Cr/Co 90/10, 12-20 mesh, (1.68 to 0.84 mm) ), prepared from chromium (III) nitrate, cobalt (II) nitrate, ammonia, ammonia nitrate (400°C) T=200 - 425°C; 9.33333 h;
参考文献
WO2004/18396 A1, ;
Page 14 ;
反应条件
bromine trifluoride; antimony(V) pentachloride in 1,2,2-trifluoro-trichloroethane T=20 - 25°C;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2276 - 2278
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2522 - 2525
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide T=200 - 425°C; 9.33333 h;
参考文献
WO2004/18396 A1, ;
Page 12-13 ;
反应条件
hydrogen fluoride; fluorine in monofluoro-trichloromethane T=-70°C; 4 h; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2012/7310 A1, ;
Page/Page column 6 ;
反应条件
nitrogen; copper; fluorine T=70°C;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3423,3425
反应条件
iodine T=140 - 165°C; 4 h;
参考文献
Yang, Zhen-Yu
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4410 - 4416
反应条件
hydrogen fluoride; 20 CrCl3 on carbon T=53 - 400°C; 4.5 h; Product distribution / selectivity;
参考文献
WO2006/69105 A1, ;
Page/Page column 14-15 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=75 - 100°C;
参考文献
US2005710 , ;
US2062743 , ;
US2005708 , ;
FR46349 ;
US2146725 , ;
反应条件
antimony (III)-antimony (V)-fluoro chloride; hydrogen fluoride; chlorine T=160 - 165°C; unter Druck;
参考文献
US2005710 , ;
US2062743 , ;
US2005708 , ;
FR46349 ;
US2146725 , ;
