1,4-二氧杂螺[4.4]壬-8-烯-7-胺合成路线 (共 3 条)
反应条件
quinoline; Lindlar's catalyst; hydrogen in ethanol
P=760 Torr; 4.5 h; Ambient temperature;
参考文献
Harris, C. John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2497 - 2502
反应条件
1: N-bromosuccinimide
2: 55 percent / NaN3, Adogen 464 / CCl4; H2O / 19 h / Ambient temperature
3: 6 percent / Lindlar catalyst, quinoline, H2 / ethanol / 4.5 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Harris, C. John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2497 - 2502
反应条件
1: 55 percent / NaN3, Adogen 464 / CCl4; H2O / 19 h / Ambient temperature
2: 6 percent / Lindlar catalyst, quinoline, H2 / ethanol / 4.5 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Harris, C. John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2497 - 2502