N-(4-氯苯基)-4-甲氧基苯甲酰胺合成路线 （共 12 条）
反应条件
samarium in acetonitrile
T=20°C; 4 h;
参考文献
Shi, Feng; Li, Jian; Li, Chunju; Jia, Xueshun
Tetrahedron Letters, 2010 , vol. 51, # 46 p. 6049 - 6051
反应条件
1,10-phenanthroline; oxygen; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in dimethyl sulfoxide
T=140°C; 72 h; Schlenk technique;
参考文献
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670,6
Title/Abstract Show Details
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670
反应条件
copper(l) iodide; manganese(II) fluoride; rel-(R,R)-DACH; potassium hydroxide in water
T=60°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Ithnin, Idzham Khalid; Yio, Siew-Hui Trionna; Lin, Zhiyin
European Journal of Organic Chemistry, 2013 , # 3 p. 515 - 524
反应条件
triethylamine; trichloromethyl chloroformate in dichloromethane
T=20°C; 0.5 h;
参考文献
Han, Ki-Jong; Tae, Beom Seok; Kim, Misoo
Organic Preparations and Procedures International, 2005 , vol. 37, # 2 p. 198 - 203
反应条件
[{(CH2SiMe2){(2,6-iPr2C6H3)N}2}Y{N(SiMe3)2}(THF)] in toluene
T=20°C; 2 h; Inert atmosphere;
参考文献
Wu, Yunjun; Wang, Shaowu; Zhang, Lijun; Yang, Gaosheng; Zhu, Xiancui; Zhou, Zhihong; Zhu, Hong; Wu, Shihong
European Journal of Organic Chemistry, 2010 , # 2 p. 326 - 332
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-70 - -20°C;
参考文献
Tandel, Sagun; Wang, Anlai; Holdeman, Terra C.; Zhang, Hongming; Biehl, Edward R.
Tetrahedron, 1998 , vol. 54, # 50 p. 15147 - 15154
反应条件
triethylamine in 1,4-dioxane
4 h; Ambient temperature;
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
1: With bis(trichloromethyl) carbonate; N,N-dimethyl-formamide in acetonitrile
Beckmann rearrangement; 5 h; Reflux;
2: With water; sodium hydrogencarbonate in acetonitrile
参考文献
Su; Zhang; Li
Organic Preparations and Procedures International, 2008 , vol. 40, # 6 p. 543 - 550
反应条件
AlCl3, aluminium chloride; formic acid; hydroxylamine hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile
T=80°C; 12 h; Schlenk technique; Overall yield = 73 percent;
参考文献
Qiu, Jun; Zhang, Ronghua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6008 - 6012
反应条件
1: methanol / Ambient temperature
2: 48 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C
3: 81 percent / triethylamine / dioxane / 4 h / Ambient temperature
View Scheme
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
