2-硝基-4，5-二甲氧基苯胺合成路线 （共 28 条）
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Descours, Denis; Festal, Didier
Synthesis, 1983 , # 12 p. 1033 - 1036
反应条件
1: 30 percent / arsenic acid, 85percent aq. phosphoric acid / 0.5 h / 100 °C
2: 80 percent / H2 / Raney nickel / ethanol / 1 h / 2327.2 Torr
View Scheme
参考文献
LaMontage, Maurice P.; Markovac, Anica; Khan, M. Sami
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 964 - 968
参考文献
The United States of America as represented by the Secretary of the Army
Patent: US4167638 A1, 1979 ;
反应条件
1: 22 percent / arsenic acid, 85percent aq. phosphoric acid / 0.5 h / 100 °C
2: 86 percent / H2 / Raney nickel / ethanol / 1 h / 2327.2 Torr
View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, vol. 77, p. 4819
反应条件
1: H2 / Raney nickel / tetrahydrofuran / 60 - 70 °C
2: triethylamine / tetrahydrofuran
3: potassium carbonate / dimethylformamide / 0.75 h / Heating
View Scheme
参考文献
Descours, Denis; Festal, Didier
Synthesis, 1983 , # 12 p. 1033 - 1036
反应条件
1: H2 / Raney nickel / tetrahydrofuran / 60 - 70 °C
2: triethylamine / tetrahydrofuran / 1 h
View Scheme
参考文献
Descours, Denis; Festal, Didier
Synthesis, 1983 , # 12 p. 1033 - 1036
反应条件
phosphoric acid; orthoarsenic acid
T=100°C; 0.5 h;
参考文献
LaMontage, Maurice P.; Markovac, Anica; Khan, M. Sami
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 964 - 968
反应条件
diarsenic pentoxide; sulfuric acid
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1542
