N-(6-羟基己基)氨基甲酸叔丁酯合成路线 （共 33 条）
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen in tert-butyl alcohol T=80°C; P=22502.3 Torr; 48 h; Autoclave;
参考文献
Ito, Masato; Koo, Lee Wei; Himizu, Akio; Kobayashi, Chika; Sakaguchi, Ayaka; Ikariya, Takao
Angewandte Chemie - International Edition, 2009 , vol. 48, # 7 p. 1324 - 1327
反应条件
in dichloromethane 12 h;
参考文献
Zeinyeh, Wael; Xia, Hexue; Lawton, Philippe; Radix, Sylvie; Marminon, Christelle; Nebois, Pascal; Walchshofer, Nadia
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 6 p. 2480 - 2488
参考文献
FUJIREBIO INC.
Patent: EP471338 A2, 1992 ;
反应条件
in tetrahydrofuran; dichloromethane
参考文献
NORTHWESTERN UNIVERSITY
Patent: US2011/177008 A1, 2011 ;
反应条件
Borane methylsulfide
参考文献
Zapf, Christoph W.; Del Valle, Juan R.; Goodman, Murray
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 18 p. 4033 - 4036
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran 2: With potassium hydroxide in tetrahydrofuran; water T=0°C;
参考文献
Osada, Satoshi; Sano, Satoshi; Ueyama, Mariko; Chuman, Yoshiro; Kodama, Hiroaki; Sakaguchi, Kazuyasu
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 2 p. 605 - 611
反应条件
zinc(II) triflate in methanol T=20°C; 0.583333 h;
参考文献
Srinivasulu; Satyanarayana; Ravi Kumar
Russian Journal of General Chemistry, 2013 , vol. 83, # 12 p. 2419 - 2422
Zh. Obshch. Khim., 2013 , vol. 83, # 12 p. 2419 - 2422,4
反应条件
sodium carbonate in tetrahydrofuran; water
参考文献
Arete Therapeutics, Inc.
Patent: US2009/270452 A1, 2009 ;
US 20090270452 A1
反应条件
2,6-dimethylpyridine; trichloromonobromomethane; Ir[(dF(CF3)ppy)2(dtbbpy)]PF6; water in acetonitrile 12 h; Inert atmosphereIrradiation; chemoselective reaction;
参考文献
Tucker, Joseph W.; Narayanam, Jagan M. R.; Shah, Pinkey S.; Stephenson, Corey R. J.
Chemical Communications, 2011 , vol. 47, # 17 p. 5040 - 5042
反应条件
in tetrahydrofuran T=60°C; 16 h;
参考文献
Menendez; Gotor
Synthesis, 1993 , # 1 p. 72 - 74
