1,4,8,11-四氮环[9.3.1.1(4,8)]十六烷合成路线 （共 10 条）
反应条件
1: 90 percent / acetonitrile / 2 h / 20 °C 2: 90 percent / NaBH4 / ethanol; H2O / 4 h / Heating View Scheme
参考文献
Royal, Guy; Dahaoui-Gindrey, Valerie; Dahaoui, Slimane; Tabard, Alain; Guilard, Roger; Pullumbi, Pluton; Lecomte, Claude
European Journal of Organic Chemistry, 1998 , # 9 p. 1971 - 1975
反应条件
1: 90 percent / acetonitrile / 24 h / 20 °C 2: aq. NaOH / 3 h View Scheme
参考文献
Kyungpook National University Industry- Academic Cooperation Foundation
Patent: EP2476683 A2, 2012 ;
反应条件
hydrogen; nickel in ethanol; ammonia T=336°C; P=98800 Torr;
参考文献
Helvetica Chimica Acta, , vol. 81, # 10 p. 1765 - 1772
反应条件
1: 90 percent / acetonitrile / 2 h / 20 °C 2: aq. NaOH / 3 h View Scheme
参考文献
Royal, Guy; Dahaoui-Gindrey, Valerie; Dahaoui, Slimane; Tabard, Alain; Guilard, Roger; Pullumbi, Pluton; Lecomte, Claude
European Journal of Organic Chemistry, 1998 , # 9 p. 1971 - 1975
反应条件
1: acetonitrile / 24 h / 20 °C 2: sodium hydroxide / 3 h 3: hydrogen / palladium-on-charcoal / ethanol / 10 h View Scheme
参考文献
Yoo, Jeongsoo; Pandya, Darpan Navinchandra
Patent: US2013/4423 A1, 2013 ;
反应条件
in water
T=0 - 20°C; 2 h; Product distribution / selectivity;
参考文献
Kyungpook National University Industry- Academic Cooperation Foundation
Patent: EP2476683 A2, 2012 ;
Location in patent: Page/Page column 27-28 ;
反应条件
formaldehyd in water
T=20°C;
参考文献
Dale, Ajit V.; Pandya, Darpan N.; Kim, Jung Young; Lee, Hochun; Ha, Yeong Su; Bhatt, Nikunj; Kim, Jonghee; Seo, Jeong Ju; Lee, Woonghee; Kim, Sung Hong; Yoon, Young-Ran; An, Gwang Il; Yoo, Jeongsoo
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 10 p. 927 - 931
参考文献
Guilard, Roger; Bessmertnykh, Alla G.; Beletskaya, Irina P.
Synlett, 1997 , vol. 1997, # 10 p. 1190 - 1192
反应条件
sodium hydroxide
8 h; Heating;
参考文献
Guilard, Roger; Bessmertnykh, Alla G.; Beletskaya, Irina P.
Synlett, 1997 , vol. 1997, # 10 p. 1190 - 1192
反应条件
hydrogen; nickel in ethanol; ammonia
T=336°C; P=98800 Torr;
参考文献
Comparone, Antonio; Kaden, Thomas A.
Helvetica Chimica Acta, 1998 , vol. 81, # 10 p. 1765 - 1772
