2,2’-(4-氨基苯基亚氨基)二乙醇合成路线 （共 8 条）
反应条件
hydrogenchloride; tin(ll) chloride in water 1 h; Heating;
参考文献
Ferlin; Via, L. Dalla; Gia
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 4 p. 771 - 777
反应条件
2: H2 / Pd-C / ethanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 82, p. 1988 - 1996
反应条件
sodium nitrite in hydrogenchloride; water
反应条件
1: 96 percent / dimethylsulfoxide / 3.5 h / Heating 2: 94 percent / HCl; SnCl2*2H2O / H2O / 1 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 4 p. 771 - 777
反应条件
potassium hexacyanoferrate(III) in water T=30°C; Rate constant;
参考文献
Palling, David J.; Brown, Keith C.; Corbett, John F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 65 - 68
反应条件
potassium hexacyanoferrate(III) in water T=30°C; effect of pH on reaction rate and effect of coupler concentration on the yield of dye studied; variuos substituted anilines and phenols; Rate constantProduct distributionMechanism;
参考文献
Palling, David J.; Brown, Keith C.; Corbett, John F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 65 - 68
反应条件
1: 1.) 1,1'-carbonyldiimidazole / 1.) DMF, 40 deg C, 30 min, 2.) 20 deg C, 10 h 2: 25 percent / SOCl2 / 1,2-dichloro-ethane / 0.5 h / Heating 3: HBr/AcOH / 4 h / 20 °C 4: 75 percent / methanol / 24 h / 20 °C View Scheme
参考文献
Gourdie; Valu; Gravatt; Boritzki; Baguley; Wakelin; Wilson; Woodgate; Denny
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1177 - 1186
反应条件
1: With water; sodium nitrite in neat (no solvent)
T=20°C;
2: With potassium iodide in neat (no solvent)
T=20°C;
参考文献
Kolvari, Eskandar; Amoozadeh, Ali; Koukabi, Nadiya; Otokesh, Somayeh; Isari, Mohsen
Tetrahedron Letters, 2014 , vol. 55, # 27 p. 3648 - 3651
