2-(2-氧代丙基)苯甲酰氯合成路线 (共 5 条)
反应条件
thionyl chloride
T=50 - 60°C; 3 h;
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: NaBH4 / methanol
2: SOCl2 / 3 h / 50 - 60 °C
3: diethyl ether
4: HCl
5: Zn/HOAc
6: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: diethyl ether
2: HCl
3: Zn/HOAc
4: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: SOCl2 / 3 h / 50 - 60 °C
2: diethyl ether
3: HCl
4: Zn/HOAc
5: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: Zn/HOAc
2: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486