alpha,alpha,2-三甲基苄醇合成路线 （共 27 条）
反应条件
1: 460 - 470 °C / beim Leiten ueber ThO2
View Scheme
参考文献
Sabatier; Murat
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 156, p. 185
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 272
反应条件
naphthalene; water; lithium
1) THF, -20 deg C, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Azzena, Ugo; Demartis, Salvatore; Melloni, Giovanni
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 4913 - 4919
反应条件
in diethyl ether
Grignard reaction; 2 h;
参考文献
Sherrill, William M.; Kim, Ryan; Rubin, Michael
Tetrahedron, 2008 , vol. 64, # 37 p. 8610 - 8617
参考文献
Tiffeneau
Annales de Chimie (Cachan, France), 1907 , vol. <8>10, p. 190
Annales de Chimie (Cachan, France), 1907 , vol. <8>11, p. 144
反应条件
lithium aluminium tetrahydride; oxygen; dibenzoyl peroxide
1.) 125 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Heinze, Antje; Lauterbach, Gerlinde; Pritzkow, Wilhelm; Schmidt-Renner, Wolfgang; Voerckel, Volkmar; Zewegsuren, Nansadyn
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 3 p. 439 - 446
反应条件
in ethanol
T=25°C; solvolysis with other solvents; Rate constant;
参考文献
Liu, Kwang-Ting; Chen, Pang-Shao; Chiu, Pao-Feng; Tsao, Meng-Lin
Tetrahedron Letters, 1992 , vol. 33, # 43 p. 6499 - 6502
参考文献
Sabatier; Murat
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 156, p. 185
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 272
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MacFaul, Philip A.; Arends, Isabella W. C. E.; Ingold, Keith U.; Wayner, Danial D. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1997 , # 2 p. 135 - 146
参考文献
Heinze, Antje; Lauterbach, Gerlinde; Pritzkow, Wilhelm; Schmidt-Renner, Wolfgang; Voerckel, Volkmar; Zewegsuren, Nansadyn
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 3 p. 439 - 446
反应条件
(i) Mg, (ii) /BRN= 635680/; Multistep reaction;
参考文献
Verkade,P.E. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1963 , vol. 82, p. 637 - 650
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
