in various solvent(s)
T=-258.2°C; 18 h; Irradiationvacuum-UV photolysis in argon matrix; IR examination of the product mixture;
参考文献
McDonald, Stephen A.; Johnson, Gary L.; Keelan, Brian W.; Andrews, Lester
Journal of the American Chemical Society, 1980 , vol. 102, # 9 p. 2892 - 2896
in various solvent(s)
T=-258.2°C; 18 h; Irradiationvacuum-UV photolysis in argon matrix; IR examination of the product mixture;
参考文献
McDonald, Stephen A.; Johnson, Gary L.; Keelan, Brian W.; Andrews, Lester
Journal of the American Chemical Society, 1980 , vol. 102, # 9 p. 2892 - 2896
silica gel in neat (no solvent)
byproducts: SiCl4, COCl2; decomposition of streaming CCl4 with high-frequency discharge in a quartz tube; condensation of the reaction mixture at -190°C; mechanism discussed; further products;; determination by IR and MS;;
参考文献
Khalafawi, T. El; Johannin-Gilles, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 242, p. 1716 - 1718
Show Details
Gmelin Handbook: C: MVol.D2, 4.1.2.7.5, page 229 - 229
in neat (no solvent)
formation of C2Cl6 and C2Cl4 at 650°C; mechanism discussed;;
参考文献
Moan, G. Le
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1962 , vol. 255, p. 2462 - 2464
Show Details
Gmelin Handbook: C: MVol.D2, 4.1.2.7.1, page 219 - 221
in neat (no solvent)
on circulating CCl4 at 650°C and 0.01-0.1 Torr in a quartz tube;;
参考文献
Moan, G. Le
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1962 , vol. 255, p. 2462 - 2464
Show Details
Gmelin Handbook: C: MVol.D2, 4.1.2.7.1, page 219 - 221