2,5-二氢-3-甲基-1-苯基膦-1-氧化物合成路线 （共 17 条）
反应条件
in tetrahydrofuran Ambient temperature;
参考文献
Li, Xinhua; Lei, Deqing; Chiang, Michael Y.; Gaspar, Peter P.
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8526 - 8531
反应条件
1: CD2Cl2 / -70 °C 2: Et3N*HCl / CH2Cl2 / 0.5 h / -70 °C 3: water / CD2Cl2 / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 629 - 634
反应条件
water in dichloromethane-d2 0.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 629 - 634
反应条件
1: dry HCl / CD2Cl2 / -50 deg C to 25 deg C 2: water / CD2Cl2 / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 629 - 634
反应条件
1: Et3N*HCl / CH2Cl2 / 0.5 h / -70 °C 2: water / CD2Cl2 / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 629 - 634
反应条件
Cu(II) stearate anschliessend Behandeln mit H2O;
参考文献
US2663737 , ;
Organic Syntheses, , vol. Coll. Vol. V, p. 787
反应条件
hydrogenchloride; water 1.) CD2Cl2, 2 days, 0 deg C, 2.) CD2Cl2, 30 min; Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 629 - 634
反应条件
sodium hydroxide; phase-transfer cat 2) heating; Multistep reaction. Title compound not separated from byproducts;
参考文献
Keglevich, Gy.; Petnehazy, I.; Toeke, L.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 51/52, p. 743
反应条件
1: 10 palladium on activated charcoal; hydrogen / methanol / 60 °C / 9375.94 Torr 2: pyridine; trichlorosilane / toluene / 2 h / 110 °C / Inert atmosphere View Scheme
参考文献
Kerenyi, Andrea; Kovacs, Viktoria; Koertvelyesi, Tamas; Ludanyi, Krisztina; Drahos, Laszlo; Keglevich, Gyoergy
Heteroatom Chemistry, 2010 , vol. 21, # 2 p. 63 - 70
反应条件
1: trichlorosilane; pyridine / toluene / 4 h / Heating 2: 0.78 g / toluene / 5 h / 20 °C 3: 49 percent / DBU / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Keglevich, Gyoergy; Forintos, Henrietta; Ujvari, Aniko; Ludanyi, Krisztina; Bitter, Istvan; Toeke, Laszlo
Journal of Chemical Research, 2005 , # 4 p. 215 - 217
