全氟(2-甲基-3-戊酮)合成路线 （共 25 条）
反应条件
1: 70 percent / sodium hypochlorite / H2O; acetonitrile 2: antimony pentafluoride / 2.5 h / 250 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 80 - 85
Zhurnal Organicheskoi Khimii, , vol. 22, # 1 p. 93 - 99
反应条件
activated carbon BAU in neat (no solvent) T=130°C; Reagent/catalystTemperature;
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 8 p. 1243 - 1251
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 8 p. 1269 - 1277,9
反应条件
1: 93 percent / sodium hypochlorite / H2O; acetonitrile 2: 94 percent / NaF / 1,2-dimethoxy-ethane / 9 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 80 - 85
Zhurnal Organicheskoi Khimii, , vol. 22, # 1 p. 93 - 99
反应条件
SbF5 T=200°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 11 p. 2285 - 2291
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2611 - 2618
反应条件
SbF5 T=250°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 80 - 85
Zhurnal Organicheskoi Khimii, , vol. 22, # 1 p. 93 - 99
反应条件
cesium fluoride in diethylene glycol dimethyl ether 2 h; Heating; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zapevalov, A. Ya.; Filyakova, T. I.; Peschanskii, N. V.; Kodess, M. I.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 1933 - 1938
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2113 - 2119
反应条件
in acetonitrile 17 h; HeatingSealed tube;
参考文献
Filyakova; Saloutina; Zapevalov; Slepukhin; Kodess; Saloutin
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 5 p. 650 - 658
反应条件
cesium fluoride in diethylene glycol dimethyl ether 1 h; Heating; Product distribution;
参考文献
Saloutina, L. V.; Filyakova, T. I.; Zapevalov, A. Ya.; Kodess, M. I.; Kolenko, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1685 - 1687
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1893 - 1896
参考文献
Fenichev; Babenko; Bispen; Moldavskii
Russian Journal of Applied Chemistry, 2013 , vol. 86, # 3 p. 376 - 386
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), 2013 , vol. 86, # 3 p. 376 - 386,10
反应条件
sodium hydroxide in water Product distribution;
参考文献
Saloutina, L. V.; Filyakova, T. I.; Zapevalov, A. Ya.; Kodess, M. I.; Kolenko, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1685 - 1687
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1893 - 1896
