全氟(2-甲基-3-戊酮)合成路线 （共 25 条）
反应条件
NAF in ethylene glycol dimethyl ether T=20°C; 9 h;
参考文献
Zapevalov, A.Ya.; Filyakova, T.I.; Kolenko, I.P.; Kodess, M.I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 80 - 85
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 1 p. 93 - 99
反应条件
cesium fluoride in ethylene glycol dimethyl ether T=50°C; 9 h;
参考文献
Zapevalov, A.Ya.; Filyakova, T.I.; Kolenko, I.P.; Kodess, M.I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 80 - 85
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 1 p. 93 - 99
反应条件
cesium fluoride in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 9.1. p. 1870 - 1876
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2057 - 2063
反应条件
bis(fluorosulfuryl) peroxide T=80°C; 192 h;
参考文献
Russian Chemical Bulletin, , vol. 47, # 12 p. 2429 - 2433
反应条件
1: hexafluorocyclopropylene oxide With potassium fluoride in diethylene glycol dimethyl ether 2 h; Heating; 2: hexafluoropropylene in diethylene glycol dimethyl ether; acetonitrile T=65 - 80°C; P=5250.53 Torr; 2 h;
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 3 p. 376 - 386
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 3 p. 376 - 386,10
反应条件
activated carbon BAU-A-2 supported 20 wtpercent CsF in neat (no solvent) T=95°C; P=1875.19 Torr;
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 8 p. 1243 - 1251
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 8 p. 1269 - 1277,9
反应条件
sodium chloride in diethylene glycol dimethyl ether 20 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, p. 1685 - 1687
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1893 - 1896
反应条件
cesium fluoride in N,N-dimethyl-formamide T=10°C; 1 h; Yield given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 9.1. p. 1870 - 1876
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2057 - 2063
反应条件
potassium fluoride in diethylene glycol dimethyl ether
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 3 p. 376 - 386
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 3 p. 376 - 386,10
反应条件
activated carbon BAU-A-2 supported 20 wtpercent CsF in neat (no solvent) T=130°C; Reagent/catalystTemperature;
参考文献
Russian Journal of Applied Chemistry, , vol. 86, # 8 p. 1243 - 1251
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), , vol. 86, # 8 p. 1269 - 1277,9
