甲基 3,4-二氢-3-氧-2H-1,4-苯噻嗪-2-醋酸酯合成路线 (共 10 条)
反应条件
acetyl chloride T=20°C;
参考文献
WO2005/92872 A1, ;
Page/Page column 28 ;
反应条件
sulfuric acid 0.166667 h; Sonication;
参考文献
Dabholkar, Vijay V.; Gavande, Rahul P.
Indian Journal of Heterocyclic Chemistry, 2011 , vol. 20, # 4 p. 359 - 364
反应条件
in neat (no solvent) T=150°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 1709 - 1711
反应条件
in neat (no solvent) T=160 - 170°C; 3 h;
参考文献
Bulletin de la Societe Chimique de France, , p. 1709 - 1711
反应条件
in methanol 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 868 - 871
反应条件
in methanol 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 868 - 871
反应条件
in methanol 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 868 - 871
反应条件
in methanol 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 868 - 871
反应条件
1: P2S5 / toluene / 0.5 h / Heating 2: neat (no solvent) / 2 h / 160 °C View Scheme
参考文献
Bourdais,J.
Bulletin de la Societe Chimique de France, 1965 , p. 1756 - 1761
反应条件
1: P2S5 / toluene / 0.5 h / Heating
2: NaOEt / ethanol / 1 h / Ambient temperature
3: neat (no solvent) / 1.5 h / 160 °C
View Scheme
参考文献
Bourdais,J.
Bulletin de la Societe Chimique de France, 1965 , p. 1756 - 1761