4-甲氧基-1-甲基吲哚合成路线 （共 11 条）
反应条件
1: 4-hydroxy-1H-indole With sodium hydride in N,N-dimethyl-formamide T=0°C; 2: methyl iodide in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Lane, Benjamin S.; Sames, Dalibor
Organic Letters, 2004 , vol. 6, # 17 p. 2897 - 2900
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Lane, Benjamin S.; Brown, Meghann A.; Sames, Dalibor
Journal of the American Chemical Society, 2005 , vol. 127, # 22 p. 8050 - 8057
反应条件
sodium hydride in tetrahydrofuran T=0 - 20°C;
参考文献
Kong, Aidi; Han, Xiuling; Lu, Xiyan
Organic Letters, 2006 , vol. 8, # 7 p. 1339 - 1342
反应条件
triethyl borane; oxygen; N-ethylpiperidinium hypophosphite in 1,4-dioxane; hexane T=73°C; 2 h; Air atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 1 p. 41 - 44
反应条件
1: sodium cyanoborohydride; acetic acid / water; acetonitrile / 12 h / 20 °C 2: triethyl borane; oxygen; N-ethylpiperidinium hypophosphite / 1,4-dioxane; hexane / 2 h / 73 °C / Air atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 1 p. 41 - 44
反应条件
1: methanol. sodium methylate / Behandeln des Reaktionsprodukts mit wss.Natronlauge 2: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the Chemical Society, , p. 3904,3909
反应条件
1: palladium; acetic acid / Hydrogenation 2: methanol. sodium methylate / Behandeln des Reaktionsprodukts mit wss.Natronlauge 3: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the Chemical Society, , p. 3904,3909
反应条件
1: aqueous HCl 2: palladium; acetic acid / Hydrogenation 3: methanol. sodium methylate / Behandeln des Reaktionsprodukts mit wss.Natronlauge 4: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the Chemical Society, , p. 3904,3909
反应条件
1: aqueous ethanol 2: aqueous HCl 3: palladium; acetic acid / Hydrogenation 4: methanol. sodium methylate / Behandeln des Reaktionsprodukts mit wss.Natronlauge 5: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the Chemical Society, , p. 3904,3909
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 3904,3909
反应条件
1: With boron tribromide in dichloromethane T=20°C; 2: With sodium hydrogencarbonate in dichloromethane; water Product distribution / selectivity;
参考文献
Cytovia, Inc.
Patent: US2006/104998 A1, 2006 ;
Location in patent: Page/Page column 20 ;
US 20060104998 A1
