carbon monoxide in methanol; acetone N2-atmosphere; addn. of LiBr (in MeOH) to Ru-complex (in Me2CO), refluxing for 5 min (pptn.), filtration off of dimethylhydrazine complex, bubbling CO (4 h) through refluxing filtrate;
参考文献
Ashworth, Terence V.; Reimann, Rolf H.; Singleton, Eric
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 1036 - 1039
in not given
treatment of Au-complex with 4-5 equiv. of LiBr, then addn. of equimolaramt. of ligand; elem. anal.;
参考文献
McAuliffe, Charles A.; Parish, R. V. (Dick); Randall, P. David
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1979 , p. 1730 - 1735