反应条件
titanium(IV) isopropylate; titanium tetrachloride
1.) CH2Cl2, -78 deg C, 1 h, 0 deg C, 2 h; 2.) H2O, DME, heating, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Miyashita; Yanami; Kumazawa; Yoshikoshi
Journal of the American Chemical Society, 1984 , vol. 106, # 7 p. 2149 - 2156
